Systematic Identification of Organic Compounds / Edition 8

by Ralph L. Shriner

Overview

Dedicated to qualitative organic chemistry, this book explains how to identify organic compounds through step-by-step instructions. Topics include elemental analysis, solubility, infrared, nuclear magnetic resonance and mass spectra; classification tests; and preparation of a derivative. Most directions for experiments are described in micro or mini scales. Discusses chromatography, distillations and the separation of mixtures. Questions and problems emphasize the skills required in identifying unknown samples.

Product Details

ISBN-13:	2900471215034
Publication date:	08/19/2003
Pages:	736
Product dimensions:	6.00(w) x 1.25(h) x 9.00(d)

About the Author

Ralph L. Shriner is the author of The Systematic Identification of Organic Compounds, 8th Edition, published by Wiley. Christine K. F. Hermann is the author of The Systematic Identification of Organic Compounds, 8th Edition, published by Wiley.

Table of Contents

Chapter 1. Introduction 1

Chapter 2. Identification of Unknowns 9

Chapter 3. Preliminary Examination, Physical Properties, and Elemental Analysis 22

Chapter 4. Separation of Mixtures 65

Chapter 5. Classification of Organic Compounds by Solubility 111

Chapter 6. Nuclear Magnetic Resonance Spectrometry 136

Chapter 7. Infrared Spectrometry 194

Chapter 8. Mass Spectrometry 228

Chapter 9. Chemical Tests for Functional Groups 247

Chapter 10. The Preparation of Derivatives 351

Chapter 11. Structural Problems—Solution Methods and Exercises 442

Chapter 12. Chemical Literature 516

Appendix I. Handy Tables for the Organic Laboratory 525

Appendix II. Tables of Derivatives 532

Appendix III. Equipment and Chemicals for the Laboratory 703

Index 711